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sp1 flash chromatography purification system  (BIOTAGE)

 
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    Structured Review

    BIOTAGE sp1 flash chromatography purification system
    Sp1 Flash Chromatography Purification System, supplied by BIOTAGE, used in various techniques. Bioz Stars score: 90/100, based on 1 PubMed citations. ZERO BIAS - scores, article reviews, protocol conditions and more
    https://www.bioz.com/product/sp1+purification+system/sp1+flash+chromatography/pmc10104803__41467_2023_37808_MOESM1_ESM-110-9-8
    Average 90 stars, based on 1 article reviews
    sp1 flash chromatography purification system - by Bioz Stars, 2026-09
    90/100 stars

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    Related Articles

    Purification:

    Article Title: Development of potent isoflavone-based formyl peptide receptor 1 (FPR1) antagonists and their effects in gastric cancer cell models.
    Article Snippet: Column chromatography was performed with 1:30 Merck silica gel 60 Å (63–200 μm) as the stationary phase. .. Flash chromatographic separations were performed on a Biotage SP1 purification system using flash cartridges pre-packed with KP-Sil 32− 63 μm, 60 Å silica. .. 1H NMR spectra were recorded on a Varian Mercury-VX spectrometer (300 MHz) or on a 500-vnmrs500 Agilent spectrometer (500 MHz).

    Article Title: Substituted imidazo[1,5-a]pyrazines for IRE1 inhibition
    Article Snippet: .. Purification by chromatography refers to purification using the COMBIFLASH® Companion purification system or the Biotage SP1 purification system. .. Where products were purified using an Isolute® SPE Si II cartridge, ‘Isolute SPE Si cartridge’ refers to a pre-packed polypropylene column containing unbonded activated silica with irregular particles with average size of 50 μm and nominal 60 Å porosity.

    Article Title: Urolithin derivatives and methods of use thereof
    Article Snippet: .. Purification by chromatography refers to purification using the COMBIFLASH® Companion purification system or the Biotage SP1 purification system. .. Where products were purified using an Isolute® SPE Si II cartridge, ‘Isolute SPE Si cartridge’ refers to a pre-packed polypropylene column containing unbonded activated silica with irregular particles with average size of 50 μm and nominal 60 Å porosity.

    Article Title: Discovery of 6-Fluoro-5-{4-[(5-fluoro-2-methyl-3-oxo-3,4-dihydroquinoxalin-6-yl)methyl]piperazin-1-yl}- N -methylpyridine-2-carboxamide (AZD9574): A CNS-Penetrant, PARP1-Selective Inhibitor.
    Article Snippet: PARP inhibitors have attracted considerable interest in drug discovery due to the clinical success of first-generation agents such as olaparib, niraparib, rucaparib, and talazoparib.. Their success lies in their ability to trap PARP to DNA; however, firstgeneration PARP inhibitors were not strictly optimized for trapping nor for selectivity among the PARP enzyme family.. Previously we described the discovery of the second-generation PARP inhibitor AZD5305, a selective PARP1-DNA trapper.

    Article Title: d-Glucose- and d-mannose-based antimetabolites. Part 4: Facile synthesis of mono- and di-acetates of 2-deoxy-d-glucose prodrugs as potentially useful antimetabolites.
    Article Snippet: 2-Deoxy-D-glucose (2-DG), a compound known to interfere with D-glucose and D-mannose metabolism, has been tested as a potential anticancer and antiviral agent.. Preclinical and clinical studies focused on 2-DG have highlighted several limitations related to 2-DG drug-like properties, such as poor pharmacokinetic properties.. To overcome this problem, we proposed design and synthesis of novel 2-DG prodrugs that subsequently could be tested using a variety of biochemical and molecular methods.

    Article Title: Structure-based design of multitargeting ChEs-MAO B inhibitors based on phenyl ring bioisosteres: AChE/BChE selectivity switch and drug-like characterization.
    Article Snippet: Column chromatography was performed using Merck silica gel 60 (0.063–0.200 mm, 70–230 mesh). .. Flash chromatographic separations were performed on Biotage SP1 purification system using flash cartridges prepacked with KP-Sil 32–63 μm, 60 Å silica. .. All reactions were routinely checked by TLC using Merck Kieselgel 60 F254 aluminum plates and visualized by UV light.

    Article Title: Deuterated N-(5-(2,3-dihydrobenzo[b][1,4]dioxine-6-carboxamido)-2-fluorophenyl)-2-((4-ethylpiperazin-1-yl)methyl)quinoline-6-carboxamide
    Article Snippet: Flash column chromatography was carried out on Merck silica gel 60 (partial size 40-65 μm). .. Column chromatography was also performed on a Biotage SP1 purification system using Biotage Flash silica cartridges (SNAP KP-Sil). .. Ion exchange chromatography was performed using acidic Isolute Flash SCX-II columns.

    Article Title: Azulene as a biphenyl mimetic in orexin/hypocretin receptor agonists.
    Article Snippet: .. When a product was purified by flash chromatography, silica gel (SiO2) 60 (230–400 mesh) or silica gel with a Biotage SP1 purification system (SNAP 10, 25, or 50 g cartridges) was used. .. Mass spectrometric analysis were performed with a Waters Synapt G2 HDMS mass spectrometer using electrospray ionization (ESI).

    Chromatography:

    Article Title: Substituted imidazo[1,5-a]pyrazines for IRE1 inhibition
    Article Snippet: .. Purification by chromatography refers to purification using the COMBIFLASH® Companion purification system or the Biotage SP1 purification system. .. Where products were purified using an Isolute® SPE Si II cartridge, ‘Isolute SPE Si cartridge’ refers to a pre-packed polypropylene column containing unbonded activated silica with irregular particles with average size of 50 μm and nominal 60 Å porosity.

    Article Title: Urolithin derivatives and methods of use thereof
    Article Snippet: .. Purification by chromatography refers to purification using the COMBIFLASH® Companion purification system or the Biotage SP1 purification system. .. Where products were purified using an Isolute® SPE Si II cartridge, ‘Isolute SPE Si cartridge’ refers to a pre-packed polypropylene column containing unbonded activated silica with irregular particles with average size of 50 μm and nominal 60 Å porosity.

    Column Chromatography:

    Article Title: Discovery of 6-Fluoro-5-{4-[(5-fluoro-2-methyl-3-oxo-3,4-dihydroquinoxalin-6-yl)methyl]piperazin-1-yl}- N -methylpyridine-2-carboxamide (AZD9574): A CNS-Penetrant, PARP1-Selective Inhibitor.
    Article Snippet: PARP inhibitors have attracted considerable interest in drug discovery due to the clinical success of first-generation agents such as olaparib, niraparib, rucaparib, and talazoparib.. Their success lies in their ability to trap PARP to DNA; however, firstgeneration PARP inhibitors were not strictly optimized for trapping nor for selectivity among the PARP enzyme family.. Previously we described the discovery of the second-generation PARP inhibitor AZD5305, a selective PARP1-DNA trapper.

    Article Title: d-Glucose- and d-mannose-based antimetabolites. Part 4: Facile synthesis of mono- and di-acetates of 2-deoxy-d-glucose prodrugs as potentially useful antimetabolites.
    Article Snippet: 2-Deoxy-D-glucose (2-DG), a compound known to interfere with D-glucose and D-mannose metabolism, has been tested as a potential anticancer and antiviral agent.. Preclinical and clinical studies focused on 2-DG have highlighted several limitations related to 2-DG drug-like properties, such as poor pharmacokinetic properties.. To overcome this problem, we proposed design and synthesis of novel 2-DG prodrugs that subsequently could be tested using a variety of biochemical and molecular methods.

    Article Title: Deuterated N-(5-(2,3-dihydrobenzo[b][1,4]dioxine-6-carboxamido)-2-fluorophenyl)-2-((4-ethylpiperazin-1-yl)methyl)quinoline-6-carboxamide
    Article Snippet: Flash column chromatography was carried out on Merck silica gel 60 (partial size 40-65 μm). .. Column chromatography was also performed on a Biotage SP1 purification system using Biotage Flash silica cartridges (SNAP KP-Sil). .. Ion exchange chromatography was performed using acidic Isolute Flash SCX-II columns.

    Article Title: Azulene as a biphenyl mimetic in orexin/hypocretin receptor agonists.
    Article Snippet: .. When a product was purified by flash chromatography, silica gel (SiO2) 60 (230–400 mesh) or silica gel with a Biotage SP1 purification system (SNAP 10, 25, or 50 g cartridges) was used. .. Mass spectrometric analysis were performed with a Waters Synapt G2 HDMS mass spectrometer using electrospray ionization (ESI).



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